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Synthesis and characterization of Epoxy Resin Amino Acid modified Organo-Clay nanocomposites.
Author(s)
Muhammad Farooq Khan Material Science Centre, School of Materials, The University of Manchester, Manchester, United Kingdom
Arthur N. Wilkinson Material Science Centre, School of Materials, The University of Manchester, Manchester, United Kingdom
John L. Stanford Material Science Centre, School of Materials, The University of Manchester, Manchester, United Kingdom
Abstract
Epoxy resin nanocomposites were prepared from diglycidyl ether of bisphenol A (DGEBA)/ 3,5-diethyltoluene diamine (DETDA) and poly(2,6-dimethyl 1,6 phenylene ether) (PPE). An organoclay, modified with 12-aminolauric acid, was dispersed in DGEBA using an ultrasonic probe. Wide angle X-ray diffraction showed an intercalated structure for the clay in the fully-reacted epoxy nanocomposites. PPE phase-separated upon curing and the resultant multiphase structure was studied using DMA. It was observed that the glass transition temperatures and rubbery moduli of fully-reacted epoxy resins increased with the addition of 10 wt % of PPE and of 5 wt % of organoclay.
Publication Details
Page(s) 139-142
DOI DOI not available
Published Journal: Proceedings 6th International Bhurban Conference on Applied Sciences and Technology , Volume: 1, Issue: 0, Year: 2009
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