Synthesis of Ammonium Persulfate/Glycerol based Novel Deep Eutectic Solvent under controlled conditions; Characterization, Physical Properties | [Sixth International Conference on Sustainability in Process Industries (SPI) 19-20 Octover 2022 (Book of Abstracts) • 2022]

Author(s):

1. Shafiq Uz Zaman: Department of Chemical Engineering, Ghulam Ishaq Khan Institute of Engineering Sciences and Technology,Topi, Khyber Pakhtunkhwa,Pakistan

2. Muhammad Shozab Mehdi: Department of Chemical Engineering, Ghulam Ishaq Khan Institute of Engineering Sciences and Technology,Topi, Khyber Pakhtunkhwa,Pakistan

3. Sikander Rafiq: Department of Chemical, Polymer and Composite Materials Engineering, University of Engineering and Technology,Lahore, New Campus,Pakistan

4. Muhammad Umar: Department of Chemical Engineering, Ghulam Ishaq Khan Institute of Engineering Sciences and Technology,Topi, Khyber Pakhtunkhwa,Pakistan

5. Saif-ur-Rehman: Department of Chemical Engineering, COMSATS University Islamabad, Lahore Campus-,,Pakistan

6. Muhammad Khaliq U Zaman: Department of Chemical Engineering, University of Gujrat,,Pakistan

Abstract:

Solvents with deep eutectic properties are characterized by decreased melting points compared to their parent components. The physicochemical properties of these materials can be tailored, which makes them ideal to be utilized for different industrial applications. They are prepared by the combination of salt with hydrogen bond donor moiety to some definite ratio. In the current study, a novel deep eutectic solvent (DES) was synthesized by the combination of ammonium persulfate and glycerol in 2:1 wt. % ratio using ramp input temperature response which otherwise resulted in uncontrolled reaction with the emission of smoke that could result in burst. The bonding behavior of synthesized novel DES was determined by FTIR spectroscopic analysis, which confirms a physiochemical combination of the constituents and leads towards the prospered synthesis of DES by the significant shifting of characteristic peaks. The physical properties such as electrical conductivity, density, viscosity, surface tension, and freezing point of the immaculate DES were also reported. The variation in physical characteristics allowed the synthesized DES to be appropriate for miscellaneous applications.

Page(s): 0-0

DOI: DOI not available

Published: Journal: Sixth International Conference on Sustainability in Process Industries (SPI) 19-20 Octover 2022 (Book of Abstracts), Volume: 0, Issue: 0, Year: 2022

Keywords:

Eutectic solvents , DES , physical properties

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