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Thermal analysis and microstructure of carbon black nanoparticles from coconut shells
Author(s):
1. Erna Frida: Department of Physics,Universitas Sumatera Utara, Medan,Indonesia
2. Bunga Fisikanta Bukit: Department of Physics,Universitas Quality Berastagi, Berastagi,Indonesia
3. Nurdin Bukit: Department of Physics,Universitas Negeri Medan, Medan,Indonesia
4. Eva Marlina Ginting: Department of Physics,Universitas Negeri Medan, Medan,Indonesia
5. Marnala Ayunita Manurung: Department of Physics,Universitas Negeri Medan, Medan,Indonesia
Abstract:
Carbon Black (CB) is widely used as a filler in rubber materials. CB has been obtained from the thermal cracking process of petroleum hydrocarbons. With the depletion of petroleum reserves, it is necessary to substitute carbon black using natural materials such as coconut shells. This research studied the thermal and microstructure properties of Coconut Shell Nanoparticles (CSNP). CSNP was synthesized by the ball mill method and coprecipitation method. Synthesis of Coconut Shell (CS) by coprecipitation method with various solvents affects the thermal properties and microstructure of the resulting carbon black. Morphological results showed that most of the carbon pores were formed, and the dominant elements in the sample were carbon and oxygen. The appearance of the absorption band, which is characteristic of CB in CS samples, was confirmed from the FTIR results. In addition, from XRD analysis, the particle size of CSNP1, CSNP2, CSNP3 samples was (33.2, 52.92, and 54.98) nm with an amorphous structure. The endothermic peak is associated with phase reduction and decomposition reactions. The thermal stability of nanoparticle coconut shells is better than coconut shells.
Page(s): 1345-1353
DOI: DOI not available
Published: Journal: ARPN Journal of Engineering and Applied Sciences, Volume: 18, Issue: 12, Year: 2023
Keywords:
Nanoparticle , Coconut Shell , carbon black , coprecipitation
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