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A facile and efficient approach to the synthesis of 2,6-Diacetylpyridine.
Author(s):
1. Guangyong Xie: Key Laboratory of Catalysis and Materials Science of Hubei Province, College of Chemistry and Materials Science, South-Central University for Nationalities, Wuhan, P.R. China
2. Haitao Ai: Key Laboratory of Catalysis and Materials Science of Hubei Province, College of Chemistry and Materials Science, South-Central University for Nationalities, Wuhan, P.R. China
3. Lu Lei: Key Laboratory of Catalysis and Materials Science of Hubei Province, College of Chemistry and Materials Science, South-Central University for Nationalities, Wuhan, P.R. China
4. Dongfang Zhang: Key Laboratory of Catalysis and Materials Science of Hubei Province, College of Chemistry and Materials Science, South-Central University for Nationalities, Wuhan, P.R. China
Abstract:
2,6-Diacetylpyridine was synthesized via esterification by using pyridine-2,6-dicarboxylic acid as precursor and successive Claisen condensation promoted by sodium for the first time. Compared with traditional sodium ethylate promoted Claisen condensation, the yield of 2,6-diacetylpyridine was improved greatly, and the procedures were simpler and convenient.
Page(s): 674-676
DOI: DOI not available
Published: Journal: Journal of Chemical Society of Pakistan, Volume: 31, Issue: 4, Year: 2009
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