An optimization on the preparation of 2, 6-diamino-3, 5-dinitropyridine. | [Journal of Chemical Society of Pakistan • 2012]

Author(s):

1. Yan Hong Wang: Department of Chemical Engineering, School of Chemical Engineering and Environment, North University of China, Taiyuan, 030051, People’s Republic of China

2. He Zhao: School of Materials Science and Engineering, Taiyuan University of Science and Technology, Taiyuan, Shanxi, 030051, People’s Republic of China

3. Zhen Hu: Department of Applied Chemistry, Faculty of Chemical Engineering, Harbin Institute of Technology, Harbin 150001, People’s Republic of China

4. Yu-Dong Huang: Department of Applied Chemistry, Faculty of Chemical Engineering, Harbin Institute of Technology, Harbin 150001, People’s Republic of China

Abstract:

An optimization on the preparation of 2, 6-diamino-3, 5-dinitropyridine (DADNP) were systematically studied. The key parameters have been systematically studied, such as the synthesis route, temperature, solvent, time, the reactant ratio, and the purification route, which influenced the purity and yield of DADNP. The optimal route was confirmed through the orthogonal experiments and would have an important reference for pilot plant scale-up.

Page(s): 936-938

DOI: DOI not available

Published: Journal: Journal of Chemical Society of Pakistan, Volume: 34, Issue: 4, Year: 2012

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Keywords are not available for this article.

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