Yield optimization for one pot synthesis of Cu, Mn based metalloporphyrin | [Journal of Chemical Society of Pakistan • 2022]

Author(s):

1. Saad Nadeem: Chemical Engineering Department, NED University of Engineering & Technology, Karachi, Pakistan.

2. Fahim Uddin: Department of Fundamental and Applied Sciences, Universiti Teknologi PETRONAS 32610 Bandar Seri Iskandar, Perak, Malaysia.

3. Maizatul Shima Shaharun: Department of Chemical Engineering,Universiti Teknologi PETRONAS 32610 Bandar Seri Iskandar, Perak, Malaysia.

4. Mohamed Ibrahim Abdul Mutalib: Chemical Engineering Department, NED University of Engineering & Technology, Karachi, Pakistan.

Abstract:

Summary: Cu and Mn based tetraphenyl porphyrin namely CuTPP and MnTPP were synthesized through a one pot route with a modified procedure and the reaction conditions (Temperature and time) were optimized based on the energy consumption during the synthesis of the target macrocyclic ligands. The temperature (145oC and 160oC) and time (3, 4, 8 hr) were used to study the effect on the product yield. The optimized values obtained using MATLAB routines are 3.7 hr and 145oC.

Page(s): 466-479

DOI: DOI not available

Published: Journal: Journal of Chemical Society of Pakistan, Volume: 44, Issue: 5, Year: 2022

Keywords:

optimization , energy , Yield , Metalloporphyrins , Macrocycle

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